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Crystal structures of the samarium amido complexes [Sm(µ-X){N(SiMe3)2}2(THF)]2 with X = Cl, Br

Title data

Karl, Marc ; Seybert, Gert ; Massa, Werner ; Agarwal, Seema ; Greiner, Andreas ; Dehnicke, Kurt:
Crystal structures of the samarium amido complexes [Sm(µ-X){N(SiMe3)2}2(THF)]2 with X = Cl, Br.
In: Zeitschrift für anorganische und allgemeine Chemie. Vol. 625 (September 1999) Issue 9 . - pp. 1405-1407.
ISSN 0044-2313
DOI: https://doi.org/10.1002/(SICI)1521-3749(199909)625:9<1405::AID-ZAAC1405>3.0.CO;2-5

Official URL: Volltext

Abstract in another language

The crystal structures of the title compounds have been determined by X-ray methods. Sm(mu-Cl) . {N(SiMe3)(2)}(2)(THF)](2) (1): Space group P2(1)/n, Z = 2, lattice dimensions at 223 K: a = 1429.5(2), b = 1302.3(3), c = 1658.6(3) pm, beta = 114.212(10)degrees, R = 0.0561. Sm(mu-Br) . {N(SiMe3)(2)}(2)(THF)](2) (2): Space group Pbca, Z = 4, lattice dimensions at 223 K: a = 1850.0(7), b = 1611.0(9), c = 1888.1(6) pm, R = 0.0497.

Further data

Item Type: Article in a journal
Refereed: Yes
Keywords: samarium; amido complexes; crystal structures
Institutions of the University: Faculties > Faculty of Biology, Chemistry and Earth Sciences > Department of Chemistry > Chair Macromolecular Chemistry II > Chair Macromolecular Chemistry II - Univ.-Prof. Dr. Andreas Greiner
Faculties
Faculties > Faculty of Biology, Chemistry and Earth Sciences
Faculties > Faculty of Biology, Chemistry and Earth Sciences > Department of Chemistry
Faculties > Faculty of Biology, Chemistry and Earth Sciences > Department of Chemistry > Chair Macromolecular Chemistry II
Result of work at the UBT: No
DDC Subjects: 500 Science > 540 Chemistry
Date Deposited: 08 Apr 2015 10:19
Last Modified: 08 Apr 2015 10:19
URI: https://eref.uni-bayreuth.de/id/eprint/9869