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Portable double-sided laser-heating system for Mössbauer spectroscopy and X-ray diffraction experiments at synchrotron facilities with diamond anvil cells

Title data

Kupenko, Ilya ; Dubrovinsky, Leonid ; Dubrovinskaia, Natalia ; McCammon, Catherine ; Glazyrin, Konstantin ; Bykova, Elena ; Boffa Ballaran, Tiziana ; Sinmyo, Ryosuke ; Chumakov, Aleksandr I. ; Potapkin, Vasily ; Kantor, Anastasia ; Rüffer, Rudolf ; Hanfland, Michael ; Crichton, Wilson A. ; Merlini, Marco:
Portable double-sided laser-heating system for Mössbauer spectroscopy and X-ray diffraction experiments at synchrotron facilities with diamond anvil cells.
In: Review of Scientific Instruments. Vol. 83 (2012) Issue 12 . - p. 124501.
ISSN 1089-7623
DOI: https://doi.org/10.1063/1.4772458

Official URL: Volltext

Project information

Project financing: Deutsche Forschungsgemeinschaft

Abstract in another language

The diamond anvil cell(DAC) technique coupled with laser heating is a major method for studying materials statically at multimegabar pressures and at high temperatures. Recent progress in experimental techniques, especially in high-pressuresingle crystalX-ray diffraction, requires portable laser heating systems which are able to heat and move the DAC during data collection. We have developed a double-sided laser heating system for DACs which can be mounted within a rather small (∼0.1 m2) area and has a weight of ∼12 kg. The system is easily transferable between different in-house or synchrotron facilities and can be assembled and set up within a few hours. The system was successfully tested at the High Pressure Station of White Beam (ID09a) and Nuclear Resonance (ID18) beamlines of the European Synchrotron Radiation Facility. We demonstrate examples of application of the system to a single crystalX-ray diffraction investigation of (Mg0.87,Fe3+ 0.09,Fe2+ 0.04)(Si0.89,Al0.11)O3perovskite (ID09a) and a Synchrotron Mössbauer Source (SMS) study of (Mg0.8Fe0.2)O ferropericlase (ID18).

Further data

Item Type: Article in a journal
Refereed: Yes
Institutions of the University: Faculties > Faculty of Mathematics, Physics und Computer Science > Group Material Sciences > Chair Crystallography
Faculties > Faculty of Mathematics, Physics und Computer Science > Group Material Sciences > Professur Materialphysik und Technologie bei extremen Bedingungen
Faculties > Faculty of Mathematics, Physics und Computer Science > Group Material Sciences > Professur Materialphysik und Technologie bei extremen Bedingungen > Professur Materialphysik und Technologie bei extremen Bedingungen - Univ.-Prof. Dr. Natalia Doubrovinckaia
Faculties
Faculties > Faculty of Mathematics, Physics und Computer Science
Faculties > Faculty of Mathematics, Physics und Computer Science > Group Material Sciences
Result of work at the UBT: Yes
DDC Subjects: 500 Science > 530 Physics
Date Deposited: 28 Jul 2015 14:01
Last Modified: 06 Jun 2017 08:29
URI: https://eref.uni-bayreuth.de/id/eprint/17197