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Free-film small-angle neutron scattering : a novel container-free in situ sample environment with minimized H/D exchange

Title data

Krauss, Sebastian W. ; Schweins, Ralf ; Magerl, Andreas ; Zobel, Mirijam:
Free-film small-angle neutron scattering : a novel container-free in situ sample environment with minimized H/D exchange.
In: Journal of Applied Crystallography. Vol. 52 (2019) Issue 2 .
ISSN 1600-5767
DOI: https://doi.org/10.1107/S1600576719000906

Project information

Project financing: SFB840

Abstract in another language

The development of a container-free sample environment which is particularly well suited for in situ reaction studies of liquid samples by small-angle neutron scattering and related techniques is reported. Hydrogen exchange with the humidity from air is reduced by an encapsulating setup in a bag filled with an inert gas such as He. The effectiveness of this measure is quantitatively accessed by infrared absorption and gravimetry, and further correlated with neutron scattering.

Further data

Item Type: Article in a journal
Refereed: Yes
Keywords: small-angle neutron scattering; SANS; free-film sample environment; hydrogen isotope exchange
Institutions of the University: Faculties > Faculty of Biology, Chemistry and Earth Sciences > Department of Chemistry > Juniorprofessur Festkörperchemie - Mesostrukturierte Materialien > Juniorprofessur Festkörperchemie - Mesostrukturierte Materialien - Juniorprof. Dr. Mirijam Zobel
Result of work at the UBT: Yes
DDC Subjects: 500 Science > 530 Physics
500 Science > 540 Chemistry
Date Deposited: 07 Mar 2019 08:41
Last Modified: 07 Mar 2019 08:41
URI: https://eref.uni-bayreuth.de/id/eprint/47857