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Preparation of Gold Nanoparticle-Poly(L-menthyl methacrylate) Conjugates via ATRP Polymerization

Title data

Gries, Katharina ; Bubel, Kathrin ; Wohlfahrt, Malte ; Agarwal, Seema ; Koert, Ulrich ; Greiner, Andreas:
Preparation of Gold Nanoparticle-Poly(L-menthyl methacrylate) Conjugates via ATRP Polymerization.
In: Macromolecular Chemistry and Physics. Vol. 212 (1 December 2011) Issue 23 . - pp. 2551-2557.
ISSN 1521-3935
DOI: https://doi.org/10.1002/macp.201100449

Official URL: Volltext

Abstract in another language

Poly(L-menthyl methacrylate) (PMenMA) is synthesized by atom transfer radical polymerization (ATRP) of methyl L-mentholacrylate using bis[2-(2-bromoisobutyrooxy)ethyl]disulfide] ((BiBOE)(2))S(2)) as the ATRP coinitiator. Reduction of hydrogen tetrachloroaureate(III) (HAuCl(4) center dot 3 H(2)O) by Super-Hydride in the presence of PMenMA yields gold nanoparticles (AuNP)-PMenMA conjugates in the size range of 220 nm, depending on the ratio of PMenMA and HAuCl(4). AuNP-PMenMA is characterized by TEM, NMR, IR-, and UV-spectroscopy. The correlation of the ratio of (AuNP)-PMenMA conjugates and free PMenMA is analyzed by gel permeation chromatography (GPC).

Further data

Item Type: Article in a journal
Refereed: Yes
Keywords: atom transfer radical polymerization; gel permeation chromatography; gold nanoparticles; menthol
Institutions of the University: Faculties > Faculty of Biology, Chemistry and Earth Sciences > Department of Chemistry > Chair Macromolecular Chemistry II > Chair Macromolecular Chemistry II - Univ.-Prof. Dr. Andreas Greiner
Faculties
Faculties > Faculty of Biology, Chemistry and Earth Sciences
Faculties > Faculty of Biology, Chemistry and Earth Sciences > Department of Chemistry
Faculties > Faculty of Biology, Chemistry and Earth Sciences > Department of Chemistry > Chair Macromolecular Chemistry II
Result of work at the UBT: No
DDC Subjects: 500 Science > 540 Chemistry
Date Deposited: 31 Mar 2015 10:30
Last Modified: 31 Mar 2015 10:30
URI: https://eref.uni-bayreuth.de/id/eprint/9520