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2D NMR characterisation of 5-norbornene-2-nonaneacidethylester and 5-norbornene-2-hexane

Title data

Müller, Kerstin ; Chun, Sung-Ho ; Greiner, Andreas ; Agarwal, Seema:
2D NMR characterisation of 5-norbornene-2-nonaneacidethylester and 5-norbornene-2-hexane.
In: Designed Monomers and Polymers. Vol. 8 (2005) Issue 3 . - pp. 237-248.
ISSN 1568-5551
DOI: https://doi.org/10.1163/1568555053993989

Official URL: Volltext

Abstract in another language

5-Norbornene-2-nonaneacidethylester and 5-norbomene-2-hexane were synthesised by Diels-Alder reaction of cyclopentadiene and corresponding olefins. Diels-Aider reaction usually results in a mixture of endo and exo isomers. The monomers were obtained in an approximate ratio of 75:25 (endo/exo), which was determined by GC-MS and H-1-NMR-spectroscopy. Both monomers were detailed characterized using ID H-1-NMR, ID C-13-NMR, 2D (1)HJH COSY, 2D H-1-C-13 HMQC and 2D H-1-C-13 HMBC techniques.

Further data

Item Type: Article in a journal
Refereed: Yes
Keywords: 2D NMR; 5-norbornene-2-hexane; 5-norbornene-2-nonaneacidethylester; Diels-Alder reaction; norbornene ester
Institutions of the University: Faculties > Faculty of Biology, Chemistry and Earth Sciences > Department of Chemistry > Chair Macromolecular Chemistry II > Chair Macromolecular Chemistry II - Univ.-Prof. Dr. Andreas Greiner
Faculties
Faculties > Faculty of Biology, Chemistry and Earth Sciences
Faculties > Faculty of Biology, Chemistry and Earth Sciences > Department of Chemistry
Faculties > Faculty of Biology, Chemistry and Earth Sciences > Department of Chemistry > Chair Macromolecular Chemistry II
Result of work at the UBT: No
DDC Subjects: 500 Science > 540 Chemistry
Date Deposited: 13 Apr 2015 08:55
Last Modified: 13 Apr 2015 08:55
URI: https://eref.uni-bayreuth.de/id/eprint/9708