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Combined Microwave and Laser Heating for Glazing of 8Y–ZrO₂ and 8Y–ZrO₂/ZrSiO₄–Composites

Title data

Richter, Christian ; Lehmann, Sebastian ; Böckler, Jens ; Willert-Porada, Monika ; Rosin, Andreas:
Combined Microwave and Laser Heating for Glazing of 8Y–ZrO₂ and 8Y–ZrO₂/ZrSiO₄–Composites.
In: Advanced Engineering Materials. Vol. 20 (2018) Issue 2 . - No. 1700912.
ISSN 1527-2648
DOI: https://doi.org/10.1002/adem.201700912

Abstract in another language

Sintered porous yttria-stabilized zirconia and zirconia composite ceramics with zirconium silicate are surface glazed by Laser-Assisted Microwave Plasma Processing (LAMPP). Suitable process parameters for surface glazing are determined for those ceramics. The plasma process is monitored by means of pyrometry and optical emission spectroscopy. In order to prove the quality of the surface glazing and to characterize hot corrosion resistance, tests with molten vanadium pentoxide are performed. After 4 h of exposure, the penetration depth of the molten salt is investigated as a function of ceramic composition and pre-treatment by glazing. Upon hot corrosion testing of glazed and non-glazed ceramics, the molten vanadium pentoxide reacts selectively with yttrium oxide, forming yttrium vanadate, and causes crack formation in the zirconia ceramics due to transition to monoclinic zirconia. The results for LAMPP-glazed ceramics show, that a surficial melting phase is achieved because process temperatures exceed 3000 °C. Hence, a dense, crack-free and hardness-enhanced surface layer achieves a better resistance to hot corrosion as compared to non-glazed ceramics. Due to LAMPP-glazing, the vanadium ingress is reduced from 33 to 7 μm for yttria-stabilized zirconia and from 104 to 17 μm for zirconia composite ceramic. Reactions and microstructural changes taking place upon LAMP-Processing are discussed.

Further data

Item Type: Article in a journal
Refereed: Yes
Additional notes: Early View = Online Version of Record published before inclusion in an issue
Institutions of the University: Faculties
Faculties > Faculty of Engineering Science
Faculties > Faculty of Engineering Science > Chair Electrochemical Process Engineering
Faculties > Faculty of Engineering Science > Former Professors > Chair Electrochemical Process Engineering - Univ.-Prof. Dr. Monika Willert-Porada
Faculties > Faculty of Engineering Science > Former Professors
Result of work at the UBT: Yes
DDC Subjects: 600 Technology, medicine, applied sciences > 620 Engineering
Date Deposited: 17 Oct 2017 09:44
Last Modified: 18 Jan 2022 11:37
URI: https://eref.uni-bayreuth.de/id/eprint/40058