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Preparation and characterization of microporous mullite-corundum refractory aggregates with high strength and closed porosity

Title data

Qi, Jiangtao ; Yan, Wen ; Chen, Zhe ; Schafföner, Stefan ; Zhou, Wenying ; Li, Guangqiang ; Wang, Qiang:
Preparation and characterization of microporous mullite-corundum refractory aggregates with high strength and closed porosity.
In: Ceramics International. Vol. 46 (2020) Issue 6 . - pp. 8274-8280.
ISSN 1873-3956
DOI: https://doi.org/10.1016/j.ceramint.2019.12.056

Abstract in another language

Four microporous mullite-corundum refractory aggregates were prepared from Al(OH)3 and kaolinite gangue through an in-situ decomposition synthesis technique. The effect of the compacting pressure (30–150 MPa) on the microstructure and strength were characterized by X-ray diffraction, scanning electron microscopy and energy dispersive spectroscopy. The higher compacting pressure limited the rearrangement of Al(OH)3 pseudomorphs during the reaction sintering process and promoted the reaction between Al(OH)3 and kaolinite gangue, leading to the formation of closed mullite layers on the surface of Al(OH)3 pseudomorphs. The pore size distributions of all four microporous aggregates were bimodal with closed pores (0.1–1.0 μm) located inside of the Al(OH)3 pseudomorphs, whereas open pores (1.0–10.0 μm) were found between the pseudomorphs. When the compacting pressure was 150 MPa, the microporous mullite-corundum refractory aggregates had a high total porosity of 40.5 %, a highly closed porosity of 16.2%, median pore size of only 0.74 μm as well as an excellent compressive strength of 103.2 MPa.

Further data

Item Type: Article in a journal
Refereed: Yes
Institutions of the University: Faculties
Faculties > Faculty of Engineering Science
Faculties > Faculty of Engineering Science > Chair Ceramic Materials
Faculties > Faculty of Engineering Science > Chair Ceramic Materials > Chair Ceramic Materials - Univ.-Prof. Dr.-Ing. Stefan Schafföner
Result of work at the UBT: No
DDC Subjects: 600 Technology, medicine, applied sciences
600 Technology, medicine, applied sciences > 620 Engineering
Date Deposited: 31 Mar 2023 10:08
Last Modified: 31 Mar 2023 10:08
URI: https://eref.uni-bayreuth.de/id/eprint/75776