Synthesis and characterization of crystalline nanosized MgF₂ powder via microemulsion route

Titelangaben

Saberi, Ali ; Negahdari, Zahra ; Bouazza, Sofiane ; Willert-Porada, Monika:
Synthesis and characterization of crystalline nanosized MgF₂ powder via microemulsion route.
In: Journal of Fluorine Chemistry. Bd. 131 (2010) Heft 12 . - S. 1353-1355.
ISSN 1873-3328
DOI: https://doi.org/10.1016/j.jfluchem.2010.09.006

Volltext

Link zum Volltext (externe URL):

Abstract

Nanosized MgF2 was synthesized by precipitation in microemulsions of water in cyclohexane stabilized by polyethylene glycol tert-octylphenyl ether. The synthesized MgF2 powder was characterized by transmission electron microscopy (TEM), scanning electron microscopy (SEM), BET specific surface area, attenuated total reflection Fourier transform infrared spectroscopy (ATR-FTIR), and X-ray diffraction (XRD). The results showed that the synthesized powder was a MgF2 powder with a crystallite size in the range of 9--11 nm and a specific surface area of 190 m2/g.